Publication details

Vsázkové technologie pro syntézu substituovaných piperazinů využívající mikrovlnný zdroj a imobilizovaný katalyzátor

Title in English Batch technology for the synthesis of substituted piperazines using a microwave source and a supported catalyst
Authors

PAZDERA Pavel ŠIMBERA Jan NĚMEČKOVÁ Dana HAVRÁNKOVÁ Eva

Year of publication 2017
Type Pilot plant, certified technology, variety, breed
MU Faculty or unit

Faculty of Science

Description A solution comprising reacting a reaction mixture containing piperazine, an electrophilic reagent and a suitable metal ion immobilized on a weak acid cation exchange reaction in a glass or PE, PP vessel in the microwave reaction chamber for a period of tens of minutes using a pulse mode 10 W. After cooling to room temperature, the reaction mixture is worked up by the usual manner.
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