Use of Mass Spectrometer for Solid Sample Analysis

• Authors: JANDERKA Pavel; CHALOUPKOVÁ Radka
• Year of publication: 2007
• Type: Article in Proceedings
• Conference: 8th Advanced Batteries and Accumulators, Book of extended abstracts
• MU Faculty or unit: Faculty of Informatics
• Field: Physical chemistry and theoretical chemistry
• Keywords: mass spectrometry;solid sample;direct inlet probe;DIP
• Description: In our contribution we present the results of solid samples analysis using mass spectrometer equipped by Solid probe introduction via direct input. This is demonstrated on the case of thermal decomposition of series of para substituted benzenediazonium salts (DAS-X). By means the off-line analysis of acquired MS data with Solid probe interface with temperature controlled chromatograms, we tried to provide more detailed analysis, determination of characteristic temperatures during heating and decomposition products.

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