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Reaction of Ph2P(CH2)(n)PPh2 (n=1, 3, 5) with elemental tellurium and comparison with members of even-numbered series
Autoři | |
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Rok publikování | 2016 |
Druh | Článek v odborném periodiku |
Časopis / Zdroj | Inorganica Chimica Acta |
Fakulta / Pracoviště MU | |
Citace | |
Doi | http://dx.doi.org/10.1016/j.ica.2016.01.015 |
Obor | Anorganická chemie |
Klíčová slova | Bis(diphenylphosphino)alkane telluride; X-ray analysis; Multinuclear NMR spectroscopy; Te-transfer |
Přiložené soubory | |
Popis | The oxidation of Ph2P(CH2)(n)PPh2 (n = 1, 3, 5) by tellurium powder was studied. The prepared compounds Ph2P(Te)(CH2)(n)P(Te)Ph-2 (1, n = 3; 2, n = 5) were characterized by P-31 and Te-125 NMR spectroscopy, elemental analysis, FTIR spectroscopy and for 2 by single-crystal X-ray analysis. (C) 2016 Elsevier B.V. All rights reserved. |