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Laser ablation synthesis of new gold carbides. From gold-diamond nano-composite as a precursor to gold-doped diamonds. Time-of-flight mass spectrometric study
Autoři | |
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Rok publikování | 2014 |
Druh | Článek v odborném periodiku |
Časopis / Zdroj | Rapid Communications in Mass Spectrometry |
Fakulta / Pracoviště MU | |
Citace | |
www | http://onlinelibrary.wiley.com/doi/10.1002/rcm.6783/abstract |
Doi | http://dx.doi.org/10.1002/rcm.6783 |
Obor | Analytická chemie, separace |
Klíčová slova | gold carbides; laser ablation synthesis; mass spectrometry; gold-doped nano-diamonds |
Popis | RATIONALE Gold carbides can be produced via laser ablation synthesis (LAS) from mixtures of nano-gold (NG) and various carbonaceous materials. The nano-composite of nano-gold (NG) and nano-diamond (ND) might represent a promising precursor for the generation of new gold carbides. METHODS Time-of-flight mass spectrometry (TOF MS), transmission electron microscopy (TEM) and energy-dispersive X-ray spectroscopy (EDX) were used. The stoichiometry of clusters was determined via modelling of the isotopic patterns and MSn analysis. |
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